HIP – Hot Isostatic Pressing

Isostatic hot pressing – elimination of porosity, maximum material density.

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What is HIP?

HIP (Hot Isostatic Pressing) is a finishing process in which the combined effect of high temperature (up to 2,000 °C) and high isostatic pressure (up to 200 MPa) in an inert atmosphere seals internal pores and cavities. The result is a density approaching 100% of the theoretical value and mechanical properties that neither standard heat treatment nor precision casting can achieve.

HIP is particularly suitable where the application cannot tolerate internal defects – in safety-critical, fatigue-loaded or corrosive environments.

How HIP works

The component entering the process has internal porosity – whether it is a casting, a sintered MIM part or a powder metallurgy component. The internal pores are not visible on the surface, but they have a significant impact on fatigue strength, toughness and stress corrosion resistance.

The HIP part is sealed inside a pressure vessel (autoclave), where it is subjected simultaneously to:

  • a temperature cycle ranging from 800 to 2,000 °C (typically 1,100–1,250 °C for steels),
  • isostatic pressure of 100–200 MPa in an inert gas (argon),
  • defined dwell times – typically 1–4 hours (the entire cycle, including heating and cooling

Pore elimination occurs via three mechanisms, which operate both sequentially and simultaneously:

  • Plastic creep – the gas pressure mechanically seals internal voids when the stress exceeds the material’s yield strength at a given temperature.
  • Creep – slow deformation of the material, which allows micropores to be reduced and eliminated.
  • Atomic diffusion – atoms migrate across the interface of a closed (collapsing) pore, resulting in a metallurgical bond between surfaces and the complete removal or minimisation of the defect.

The result is a component free of internal porosity with a density close to 100% of the theoretical value. The external dimensions vary depending on the initial porosity of the material prior to HIP.

The HIP process is isotropic – pressure is applied uniformly from all sides. During the process, high temperatures may cause microstructural changes that can lead to a reduction in anisotropy; however, this is primarily determined by the material’s structure and may not be completely eliminated.

Parts processed using HIP technology

From castings for the aerospace industry to MIM sintered parts for the healthcare sector. We apply HIP treatment to parts made of steel, titanium, nickel superalloys and ceramic components. We will assess the suitability of your component and propose the process parameters.

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The HIP process, step by step

Six steps from powder to the finished part. Every single one takes place under our own roof.

1. Receipt and incoming inspection of parts

Each part enters the process accompanied by documentation detailing the material batch. We carry out a visual inspection, a dimensional analysis and a density measurement.

2. HIP cycle proposal

Based on the material, geometry and the customer’s application requirements, we design the cycle parameters: temperature, pressure, dwell time, and heating and cooling rates. We work with certified cycles whilst also developing our own sets of parameters for non-standard alloys.

Commonly used material groups for HIP treatment:

Material group Typical alloys / materials Typical applications
Low- and medium-alloy steels 4140 (DIN 1.7225), ČSN 15 142 Machine parts, moulds, forgings
Stainless and duplex steels 316L, 17-4PH, 2205 Chemical industry, healthcare
Tool steels M2, H13, ČSN 19 830 Moulds, cutting tools, cylinders
Aluminium alloys AlSi10Mg, AlSi7Mg, AlSi12 Castings, aerospace components
Titanium alloys Ti-6Al-4V, Ti-6Al-2Sn-4Zr-2Mo Aerospace, healthcare, motorsport
Nickel and cobalt superalloys Inconel 718, 625, Waspaloy, CoCr Aviation engines, turbines, medicine
Ceramics and cermets Al₂O₃, ZrO₂, Si₃N₄, WC-Co Cutting inserts, ballistic protection

3. Placing in the autoclave

The parts are placed on loading beams and loaded into the pressure chamber of the Quintus QIH 21 unit. The chamber capacity and loading flexibility allow batches ranging from single parts to hundreds of parts to be processed at once. Parts made from different materials can be combined in a single load, provided that the cycle compatibility conditions are met.

4. The HIP cycle

Once the autoclave has been hermetically sealed, the following takes place:

  • A controlled increase in temperature according to a defined profile
  • Pressurisation to working pressure (100–200 MPa) using argon
  • Holding at the working temperature and pressure (typically 1–4 hours)
  • Controlled cooling in accordance with the material’s heat treatment

The HIP process is controlled by a control system that monitors and regulates the temperature, pressure and time profile of the entire cycle. Thanks to this control, precisely defined properties of the final product can be achieved.

5. Final inspection

Following the HIP cycle, it is possible to carry out dimensional analysis, determine density and, for critical applications, also perform metallographic analysis and defectoscopy to detect surface and subsurface defects, or determine mechanical properties on test specimens from the same batch.

6. Post-processing and dispatch

We can provide – in the same way as for MIM – a complete post-processing service:

  • Machining of precision functional surfaces
  • Thermal and chemical-thermal treatments – heat treatment, ageing, nitriding
  • Surface treatments – passivation, PVD, DLC, electroplating
  • Non-destructive testing and certification in accordance with customer standards (AMS, ASTM, EN)
HIP konzole

PM HIP – direct consolidation of powders into near-net-shape components

HIP is not merely a finishing process. In PM HIP (Powder Metallurgy HIP) mode, it serves as a primary manufacturing method: metal powder is poured into a steel mould shaped like the final component, evacuated, hermetically sealed and processed in a HIP furnace.

PM HIP enables the production of both small and large components for which a fine-grained microstructure and isotropic properties would otherwise be unattainable – for example, valve bodies for the oil industry weighing up to 30 tonnes, aircraft fuselage rings or rocket engine components. The resulting shape is near-net shape, so material waste and the extent of machining are minimal.

Where HIP delivers results

The greatest benefits of HIP are seen in materials and technologies where closed pores are formed (casting, MIM, PM, AM) and in critical applications where internal defects are a limiting factor on service life.

Purity 99.9%

Standard sintering in MIM achieves 95–98 % of the theoretical density. The remaining 2–5 % consists of closed pores, which are preferred sites for the initiation of fatigue cracks. HIP eliminates these defects by diffusion sealing – the resulting microstructure is compact, homogeneous and virtually free of internal porosity detectable metallographically.

Density ≥ 95%

Density and strength comparable to those of forged material. Density ≥ 95 % of the theoretical value. Unlike piston pressing (85–90 %), MIM achieves properties that can be used in structural calculations without the need for correction factors for porosity.

4–5 times greater strength

Fatigue strength 4–5 times higher than with standard heat treatment. For nickel superalloys (Inconel 718) and titanium alloys (Ti-6Al-4V), certified material tests show a 4–5-fold increase in fatigue life following HIP treatment compared with parts that have undergone heat treatment alone. For aerospace and medical applications, this is a key parameter, not merely a marketing claim.

Compatibility

Compatibility with MIM, powder metallurgy (PM) compaction and precision casting. HIP is a finishing process that is widely applicable across various manufacturing technologies. It can be used for parts produced using MIM, powder metallurgy (PM compaction), precision casting and additive manufacturing (SLM/LPBF). In all cases, internal defects are sealed and mechanical properties are improved.

Processing of ceramics and cermets

HIP is not exclusively a metallurgical process. Ceramic components (Al₂O₃, ZrO₂, Si₃N₄) and cermets (WC-Co) achieve higher flexural strength and crack propagation resistance following HIP treatment. Applications include ballistic protection, cutting inserts, bearings and medical implants.

Reduction in variance

Reduction in the variation of mechanical properties – lower safety factors. HIP eliminates the so-called ‘scatter band’ – the variation in mechanical properties caused by an inhomogeneous internal structure. A designer working with a HIP-treated component can apply lower safety factors and design a lighter component without compromising reliability. For applications in the aerospace and medical sectors, this is a direct economic and weight-saving advantage.

Diffusion bonding (HIP cladding)

Diffusion bonding (HIP cladding) – bimetallic components without welds. HIP enables two different materials to be bonded together through diffusion – for example, a layer of corrosion-resistant Inconel or Stellite onto a low-cost carbon steel core. The bond is formed without a heat-affected zone, without the risk of cracks and without the use of filler material. The resulting strength of the joint is higher than that achieved with conventional weld overlay. Typical applications: pipe fittings, pumping components for the chemical industry, tool coatings on dies.

VIBROM operates a Quintus QIH 21 HIP system in-house. The customer does not have to worry about selecting an external supplier, transporting parts or uncertainty regarding delivery times.

HIP or another method?

HIP vs. standard heat treatment

Hardening, annealing and tempering optimise the phase composition and eliminate internal stresses – but they do not seal internal pores. HIP achieves both simultaneously: with a correctly selected cycle, heat treatment and densification take place in a single operation. For nickel superalloys and titanium alloys, the combined HIP cycle (HIP + solution annealing + ageing) is the standard in the aerospace industry.

HIP vs. repeated remelting

Remelting (vacuum or electroslag) improves the chemical homogeneity of the ingot, but inevitably alters its geometry – the semi-finished product must be machined again. HIP preserves the shape of the component and seals defects exactly where they are, without the need for further machining.

HIP vs. impregnation (resin sealing)

Impregnating the pores with resin is a quick and inexpensive solution for ensuring leak-tightness under fluid pressure. However, it does not improve the mechanical properties – fatigue strength and toughness remain unchanged. HIP seals the pores with the metal material itself.

Who uses HIP technology?

HIP technology is used by companies that manufacture components requiring high levels of structural integrity, defined mechanical properties and repeatability, in both single-piece and mass production.

Aerospace and defence industry

  • turbine blades
  • structural castings
  • airframe structural components

AS9100 requirements, AMS specifications, certified HIP cycle.

Medicine and Healthcare

  • orthopaedic implants made from Ti-6Al-4V and CoCr alloys
  • dental components

HIP as a prerequisite for biocompatibility and long-term fatigue resistance within the patient’s body.

Energy and Petrochemicals

  • rotors
  • pump housings
  • valve blocks

Nickel superalloys and duplex steels. Resistance to stress corrosion cracking.

Electronics and Electrical Engineering

  • connecting rods
  • pistons for internal combustion engines
  • Ti and Inconel turbines

HIP as a means of maximising reliability whilst minimising weight.

Industrial tools and moulds

  • M2 and H13 tool steels

HIP treatment increases the tool’s fatigue resistance under cyclic loading.

Powder metallurgy and MIM

Standard post-processing for components requiring maximum density and fatigue strength – without the need to seek an external HIP supplier.

Typical components processed using the HIP method

  • Turbine blades and distributor wheels made from Inconel, Waspaloy and titanium alloys
  • Structural castings for aircraft airframes – sub-assemblies, engine mounts
  • Orthopaedic implants – hip and knee replacements, spinal implants
  • Dental abutments and crowns made from CoCr and ZrO₂
  • Turbochargers and turbines for motorsport
  • Pump housings and valves for the chemical industry
  • Tool steels – die-casting moulds, die-cutting tools
  • MIM components requiring maximum fatigue strength
  • Ceramic ballistic components and WC-Co cutting inserts
  • Additively manufactured parts (SLM/LPBF) – elimination of internal porosity post-printing

Comparison table – HIP vs. the main alternatives

Parameter HIP (completion) PM HIP Standard TZ Fittings Impregnation
Sealing of internal pores yes Yes no no surface only
Improvement in fatigue strength +300–400 % high no medium no
Isotropy of properties absolute absolute high medium no
Geometric stability depending on the porosity of the input material Near-net shape yes machining required yes
Material utilisation ~90 % ~90 % ~100% ~60–70 % ~100 %
Tolerance ±0.1% ±0.1% - ±0.5 % -
Suitability for ceramics / cermets yes no no no no
Achievable density ≥ 99.9% ≥ 99.9% 95–98 % 99%+ ~95% (surface)
Max. part weight depending on the equipment depending on the machine unlimited unlimited unlimited
Parameter Value
Operating temperature 800–2,000 °C (typically 1,100–1,250 °C for steels)
Operating pressure 100–200 MPa (isostatic)
Working medium Argon (inert atmosphere)
Achievable density ≥ 99.9% of the theoretical value
Dimensional change after HIP depending on the porosity of the input material
Cycle duration 8–24 hours (including heating and controlled cooling)
Equipment Quintus QIH 21 (in-house)
Material compatibility Steels, titanium, nickel/cobalt superalloys, ceramics, cermets
PM HIP – maximum part weight depending on the equipment
Heat treatment in a cycle Possible (combined HIP cycle and others)
Process certification AMS 2801, AMS 7000, ASTM F3122, EN 9100
Batch traceability From raw material to HIP cycle report

Why Vibrom?

Our own Quintus QIH 21 HIP equipment – in-house

We carry out isostatic hot pressing in-house, using our own industrial equipment. The customer does not need to worry about finding an external partner or arranging the transport of parts to a third party. Delivery times are under our control.

The complete MIM → HIP process chain

For customers who have us manufacture MIM parts, HIP is a natural next step requiring no external collaboration. We take full responsibility for the final part – from the feedstock through to the HIP protocol and the final certificate.

Certified cycles and the development of custom parameters

We work with certified HIP cycles in accordance with AMS and ASTM standards. At the same time, we develop our own sets of parameters for non-standard alloys in collaboration with research institutions – including the Czech Academy of Sciences.

Defectoscopy and full batch documentation

Each batch is documented: temperature and pressure logs, dimensional measurements before and after processing, and metallographic analysis of a representative sample. For aerospace and medical applications, we carry out X-ray or ultrasonic non-destructive testing as a standard part of the process.

ISO 9001

Traceability from the batch of input material through to dispatch. The quality management system covers the entire process chain. Every component is identifiable throughout the entire manufacturing process.

Design to cost

We are involved in the design of the part to eliminate unnecessary costs even before the mould is manufactured. Changing the geometry in a PDF is inexpensive; changing it in the mould is not.

What you might find interesting about HIP

HIP is economically viable when internal porosity significantly affects the performance or reliability of a component. Typical examples include: components subjected to cyclic or dynamic loading (fatigue), components for the aerospace or medical industries, and castings made from superalloys or titanium alloys.

CIP operates at room temperature and is used to compact powders prior to sintering – it is a forming process, not a method of eliminating internal porosity. HIP combines heat and pressure to seal defects by diffusion – it is applied to parts that have already been sintered or cast.

Yes. The combined HIP cycle (HIP + solution annealing + ageing) is the standard approach in the aerospace industry. It saves one heat treatment and ensures uniform properties throughout the entire component.

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